THAT1512 / Transformer 'blind test' mic preamp

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Not sure how your scope works but can it do a trigger view with the trigger source set to line? That might reveal your mains waveform safely. With no further clues, I suspect your mains is flat topped unless your transformer is saturating. It should not saturate with no load, I’d think. I could be wrong though.
 
@DaveDC Yes, good idea, I'll do this when I get the chance, possibly tomorrow.

It's driving me a bit mad now because I can't see what's wrong with the design, it should work. I've built lots of linear power supplies before and never had so many problems. 😅 Anyway, it's the name of the game with DIY electronics!
 
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